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Malvern Panalytical Scientific Award 2023

Our 2023 Scientific Award is now open – and there’s a €5,000 prize for the best entry.
Entries close August 31st – you’ve still got time!

QUESTION

What is the matrix effect in XRF?

The matrix effect in XRF is the influence that the sample’s overall composition has on the X-ray signal from individual elements. It can cause some element signals to be absorbed or enhanced by other elements in the sample, which affects reported concentrations.

Why Matrix Effects Matter in XRF Measurements

XRF does not measure elements in isolation. It measures fluorescent X-rays emitted from a sample, and those X-rays must pass through the surrounding material before reaching the detector. If the sample contains elements or compounds that strongly absorb certain X-ray energies, the signal from some elements may be reduced.

The opposite can also occur. One element may emit X-rays that excite another element, increasing its measured signal. This enhancement can make a concentration appear higher unless the analyser software applies suitable correction models.

Matrix effects are especially important in ores, soils, powders, slurries, complex alloys, and other mixed materials. Calibration selection, sample preparation, particle size, moisture, and sample homogeneity all help determine how well matrix effects are controlled. For reliable results, the analyser should be matched to the material type and used with appropriate methods for the application.

Evaluating XRF for Complex Samples

For more detail on how the method works, review PAS’s overview of X-Ray Fluorescence technology. To compare field-ready instruments, explore PAS’s handheld XRF analysers through Portable Analytical Solutions, or contact our team to discuss your sample type and measurement requirements.

WANT MORE INFO?

Want to find out more? Reach out to our team today, and we’ll be more than happy to help.

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