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Malvern Panalytical Scientific Award 2023

Our 2023 Scientific Award is now open – and there’s a €5,000 prize for the best entry.
Entries close August 31st – you’ve still got time!

QUESTION

What is the role of chemometric calibration in NIR?

Chemometric calibration is the process that allows NIR spectra to be converted into useful analytical results. It uses mathematical models to relate spectral patterns to known reference values, such as moisture, protein, composition, or material identity.

How Chemometrics Turns NIR Spectra into Results

NIR spectra contain broad, overlapping absorption features rather than simple isolated peaks. Chemometric calibration is used to interpret this complex spectral information and link it to the property being measured.

A calibration model is built using representative samples that have been analysed by a reliable reference method. The NIR spectra and reference results are then used to create a model that can predict results for similar unknown samples.

The quality of the calibration controls the reliability of the NIR result. A good model should include the expected range of sample variation, including composition, moisture, particle size, temperature, and presentation conditions. Models also need validation to confirm they perform reliably on real samples, not only on the calibration set.

Building Confidence in NIR Calibration

For more detail on the measurement principle, review PAS’s overview of Near Infrared Spectroscopy technology. To compare suitable systems, explore PAS’s NIR analysers through Portable Analytical Solutions, or get in touch to discuss calibration models, reference data, and application requirements.

WANT MORE INFO?

Want to find out more? Reach out to our team today, and we’ll be more than happy to help.

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